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Extraction of Limonene from Orange Peels Through Steam Distillation
Conclusion
Recommendations
- Run analysis right away
- Grapefruits, lemons, limes
Questions
Analysis of Product
Buffer
Refractive Indices
Analysis of Product
Citrate Buffer (pH 4.95)
Phosphate Buffer (pH 6.86) 1.3323 - 1.3360
Water (pH 7.42)
Phosphate Buffer (pH 7.90) 1.470-1.474
IR Spectra
Percent Yield
Reference:
Limonene - 1.4730
Water - 1.34
IR Spectrum of Product from Citrate Buffers,
Phosphate Buffer (pH 6.86), & Water Trials
IR Spectrum of Water (Reference)
IR Spectrum of Product from Phosphate Buffer (pH 7.90) Trials
IR Spectrum of Limonene (CRM)
Citrate Buffer (pH 4.95) 54%
Citrate Buffer (pH 5.82) 33%
Phosphate Buffer (pH 6.86) 1.2%
Phosphate Buffer (pH 7.90) 0.91%
Water (pH 7.42) 2.9%
Buffers
Citrate Buffer Solution pH 4.95
Citrate Buffer Solution pH 5.82
Phosphate Buffer Solution pH 6.86
Phosphate Buffer Solution pH 7.90
Water pH 7.42
Background
Limonene
- essential oil from citrus fruits
Steam Distillation
- separation method